Position | δC EXP | δC LIT.a | δH EXP | δH LIT.b |
---|---|---|---|---|
1 | 38.4 | 38.5 | Â | Â |
2 | 31.9 | 32.1 | Â | Â |
3 | 70.5 | 70.5 | 3.64Â m (1H) | 3.61Â m (1H) |
4 | 40.8 | 40.9 | Â | Â |
5 | 139.8 | 139.8 | Â | Â |
6 | 119.6 | 119.7 | 5.58 dd (5.5, 3.0Â Hz, 1H) | 5.56 dd (5.4, 2.2Â Hz, 1H) |
7 | 116.3 | 116.4 | 5.38 dd (5.4, 2.9Â Hz, 1H) | 5.38 dd (5.4, 2.5Â Hz, 1H) |
8 | 141.4 | 141.3 | Â | Â |
9 | 46.2 | 42.3 | Â | Â |
10 | 37.1 | 37.1 | Â | Â |
11 | 21.1 | 21.1 | Â | Â |
12 | 39.1 | 39.1 | Â | Â |
13 | 42.9 | 42.9 | Â | Â |
14 | 54.6 | 54.6 | Â | Â |
15 | 22.9 | 23.1 | Â | Â |
16 | 28.3 | 28.3 | Â | Â |
17 | 55.7 | 55.8 | Â | Â |
18 | 12.1 | 12.1 | 0.95Â s (3H) | 0.95Â s (3H) |
19 | 16.3 | 16.3 | 0.65Â s (3H) | 0.63Â s (3H) |
20 | 40.3 | 40.4 | Â | Â |
21 | 21.1 | 21.2 | 1.04 d (J = 6.6 Hz, 3H) | 1.00 d (J = 6.6 Hz, 3H) |
22 | 135.6 | 135.6 | 5.20Â m (1H) | 5.20Â m (1H) |
23 | 131.9 | 132.1 | 5.21Â m (1H) | 5.20Â m (1H) |
24 | 42.9 | 42.9 | Â | Â |
25 | 33.1 | 33.1 | Â | Â |
26 | 19.9 | 20.0 | 0.84 d (J = 6.7 Hz, 3H) | 0.84 d (J = 6.7 Hz, 3H) |
27 | 19.7 | 19.7 | 0.82 d (J = 6.7 Hz, 3H) | 0.83 d (J = 6.7 Hz, 3H) |
28 | 17.6 | 17.6 | 0.92 d (J = 6.6 Hz, 3H) | 0.95 d (3H) |