Table 2 Mass fingerprint of crude venom from X. appendiculata circumvolans
From: Peptidomic analysis of the venom of the solitary bee Xylocopa appendiculata circumvolans
Fraction no. | Retention time (min) | [M + H]+ m/z |
|---|---|---|
1 | 1.0–1.5 | 116.071, 175.119, 184.073, 348.071, 381.080, 405.236, 441.101 |
2 | 1.5–2.0 | 132.102, 268.104, 322.077, 377.058, 733.323, 759.499 |
3 | 2.0–3.0 | 284.099, 373.281, 437.051, 469.277, 654.357, 817.504, 947.484, 1002.508 |
4 | 3.0–4.2 | 182.117, 431.214, 598.428, 937.390, 1368.747 |
5 | 4.2–5.0 | 623.423, 646.423, 1517.714, 2064.031 |
6 | 5.0–6.0 | 930.588, 969.653, 1165.500, 1189.459, 1338.913, 1306.915, 1715.808, 2807.314 |
7 | 6.0–6.4 | 322.176, 393.214, 961.656, 1210.815, 1451.994, 1925.941 |
8 | 6.4–7.0 | 714.306, 1211.799, 1268.821, 1336.563, 1510.001, 3225.624, 3243.642 |
9 | 7.0–8.0 | 637.346, 715.291, 793.482, 838.421, 875.527, 1082.720, 1178.861, 1337.549, 1565.078, 1636.116, 2064.036, 3400.643 |
10 | 8.0–9.0 | 690.456, 747.477, 908.509, 933.515, 937.678, 1249.897, 1427.606, 1608.000, 1626.012, 1694.121, 2065.019, 3187.725, 3245.730 |
11 | 9.0–10.0 | 379.114, 506.298, 696.502, 761.492, 988.656, 1021.593, 1085.709, 1366.821, 1384.832, 1882.253, 3187.723, 3245.728 |
12 | 10.0–10.8 | 370.199, 941.598, 1690.115, 1735.185, 1939.274 |
13 | 10.8–11.4 | 619.381, 926.118, 1553.055, 1783.363, 1997.276 |
14 | 11.4–12.0 | 1311.877, 1803.199, 1899.267, 2087.312, 2139.353, 2236.641, 3087.760, 3256.821 |
15 | 12.0–12.7 | 680.314, 704.272, 1424.961, 1956.252, 2121.345, 2197.359, 2281.379, 2648.565 |
16 | 12.7–13.2 | 2095.280, 2113.292 |
17 | 13.2–13.6 | 662.303, 1316.450, 2077.267, 2153.287, 2171.297 |
18 | 13.6–15.0 | 1709.063, 3860.509, 4015.525 |